In-situ Structure Characterization of Elastomers during Deformation and Fracture
Seiten
2016
|
1. Softcover reprint of the original 1st ed. 2014
Springer International Publishing (Verlag)
978-3-319-36034-8 (ISBN)
Springer International Publishing (Verlag)
978-3-319-36034-8 (ISBN)
This thesis offers novel insights into the time-dependent structural evolution of polymers under deformation. In-situ tensile experiments at high-brilliance synchrotron sources allowed to characterize the material with unrivaled resolution in time and space. The strain-induced crystallization in natural rubber was studied by wide-angle X-ray diffraction. Special emphasis was put on the establishment of new structure-property relationships to give a more in-depth understanding of the mechanical performance of rubber parts, e.g. in tear fatigue loading. To this end, the kinetics of strain-induced crystallization were investigated, subjecting the material to high strain rates. The local structure around a crack tip was observed by scanning wide-angle X-ray diffraction. Ultra-small angle X-ray scattering served to study filled elastomers under deformation, from specially prepared model filler systems to industrially relevant carbon black filled rubbers. Other methods include electron microscopy coupled with in-situ tensile testing and optical dilatometry to examine cavitation in rubbers.
The underlying theory as well as a literature review are covered by an extensive introductory chapter, followed by a description of the experimental techniques. The results are presented in more detail than in the original journal publications.
The underlying theory as well as a literature review are covered by an extensive introductory chapter, followed by a description of the experimental techniques. The results are presented in more detail than in the original journal publications.
Introduction.- Motivation and Objectives.- Experimental.- Results.- Conclusion and Outlook.- Appendix.
| Erscheinungsdatum | 16.09.2016 |
|---|---|
| Reihe/Serie | Springer Theses |
| Zusatzinfo | XIV, 124 p. 82 illus., 51 illus. in color. |
| Verlagsort | Cham |
| Sprache | englisch |
| Maße | 155 x 235 mm |
| Themenwelt | Naturwissenschaften ► Chemie ► Organische Chemie |
| Technik ► Maschinenbau | |
| Schlagworte | Cavitation • Ceramics, Glass, Composites, Natural Methods • Characterization and Evaluation of Materials • Chemistry • Chemistry and Materials Science • Condensed matter physics • Crystallization Kinetics • Elastomer Deformation and Fracture • Industrial chemistry and chemical engineering • materials / states of matter • Mechanical Properties of Polymers • Natural Rubber Reinforcement • polymer chemistry • Polymer sciences • Polymers Under Deformation • Strain-induced Crystallization • Synchrotron Small and Wide-Angle X-ray Scattering • Synchrotron Small and Wide-Angle X-ray Scattering & Diffraction • Synchrotron X-ray Radiation • Testing of materials • Time-dependent Structure Evolution in Polymers • WAXD, SAXS, USAXS, SEM |
| ISBN-10 | 3-319-36034-5 / 3319360345 |
| ISBN-13 | 978-3-319-36034-8 / 9783319360348 |
| Zustand | Neuware |
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Buch | Softcover (2021)
Wiley-VCH (Verlag)
CHF 23,80
