Equipment and Process Design for Small-scale Continuous Crystallization
Seiten
2019
Dr. Hut (Verlag)
9783843941167 (ISBN)
Dr. Hut (Verlag)
9783843941167 (ISBN)
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Continuous processing and modularization offer opportunities for an enhanced resource and energy efficiency, a stable product quality and reduced time-to-market in production processes in the fine chemical and pharmaceutical industries which are conventionally based on batch manufacturing. The shift to a fully continuous production in these branches requires suitable continuous flow equipment and versatile design concepts for a variety of product properties and process conditions.
This study focusses on cooling crystallization from solution as being an important work-up and product purification method for a large variety of fine chemicals and pharmaceuticals. The design of a continuous tubular cooling crystallizer is presented, starting with a design concept followed by the manufacturing and characterization of a laboratory level prototype for the g/h scale. The equipment concept is based on horizontal helical coil tubes in the coiled flow inverter (CFI) design. The scale-up of the CFI cooling crystallizer concept to miniplant level and kg/h scale is successfully demonstrated. The developed equipment concepts and methods enable the design and scale-up of robust continuous flow tubular equipment for a variety of solid-liquid processes.
This study focusses on cooling crystallization from solution as being an important work-up and product purification method for a large variety of fine chemicals and pharmaceuticals. The design of a continuous tubular cooling crystallizer is presented, starting with a design concept followed by the manufacturing and characterization of a laboratory level prototype for the g/h scale. The equipment concept is based on horizontal helical coil tubes in the coiled flow inverter (CFI) design. The scale-up of the CFI cooling crystallizer concept to miniplant level and kg/h scale is successfully demonstrated. The developed equipment concepts and methods enable the design and scale-up of robust continuous flow tubular equipment for a variety of solid-liquid processes.
| Erscheinungsdatum | 16.08.2019 |
|---|---|
| Reihe/Serie | Thermodynamik |
| Verlagsort | München |
| Sprache | englisch |
| Maße | 148 x 210 mm |
| Gewicht | 268 g |
| Themenwelt | Naturwissenschaften ► Physik / Astronomie ► Thermodynamik |
| Technik | |
| Schlagworte | Continuous processing • crystallization • Tubular Device |
| ISBN-13 | 9783843941167 / 9783843941167 |
| Zustand | Neuware |
| Informationen gemäß Produktsicherheitsverordnung (GPSR) | |
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