Techniques Labs for Macroscale and Microscale Organic Experiments

Kenneth Williamson, Katherine M. Masters (Autoren)

Media-Kombination

336 Seiten

2011 | 6th Revised edition
CENGAGE Learning Custom Publishing
978-1-111-43041-2 (ISBN)

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Offering a flexible mix of macroscale and microscale options for most experiments, this title emphasizes safety and allows users to save on the purchase and disposal of expensive, sometimes hazardous, organic chemicals.

This manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. Featuring updated NMR spectra, new experiments that stress green chemistry and a Premium Website that includes glassware-specific videos with pre-lab, gradable exercises, this TECHNIQUES LABS edition of the authors' proven lab manual includes the most commonly used labs in the print manual and makes all the other experiments from MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS available for download on the companion website. Offering a flexible mix of macroscale and microscale options for most experiments, this proven manual emphasizes safety and allows users to save on the purchase and disposal of expensive, sometimes hazardous, organic chemicals. Macroscale versions can be used for less costly experiments, allowing users to get experience working with conventionally-sized glassware.

Ken Williamson is retired from Mt. Holyoke College where he taught the organic chemistry laboratory course. He is an established authority on microscale techniques and regularly holds workshops and travels to campuses in the U.S., Canada, and Europe to demonstrate the use of microscale. A PhD from Pennsylvania State University, Katherine Masters is director of the organic chemistry laboratory courses at Penn State.

1. Introduction. 2. Laboratory Safety, Courtesy, and Waste Disposal. 3. Melting Points and Boiling Points. 4. Recrystallization. 5. Distillation. 6. Steam Distillation, Vacuum Distillation, and Sublimation. 7. Extraction. 8. Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste. 9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments. 10. Gas Chromatography: Analysis of Alkene Isomers. 11. Infrared Spectroscopy. 12. Nuclear Magnetic Resonance Spectroscopy. 13. Mass Spectroscopy. 14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis. 15. Computational Chemistry.

Erscheint lt. Verlag	1.1.2011
Verlagsort	Mason, OH
Sprache	englisch
Maße	217 x 276 mm
Gewicht	724 g
Themenwelt	Naturwissenschaften ► Chemie ► Organische Chemie
ISBN-10	1-111-43041-1 / 1111430411
ISBN-13	978-1-111-43041-2 / 9781111430412
Zustand	Neuware